Complete kit for HNO3 production via Birkeland-Eyde process.
It
is a kit to assemble yourself by following the steps in the PDF below,
which will allow you to produce within 20g of HNO3 per day (more or
less according to the building factors) while consuming around 50
watts.
I can guarantee you to get nitric acid, but the amount
per unit of time depends on many parameters like gap space between
electrodes, the distance of input fresh air from arc, level of water
in the bubbler tank, etc.
Mounting :
This
equipment requires some little DIY skills, read the instructions in
the PDF before please.
No specific tools are needed, only common
ones like cutter, scissors…
Due to the little amount of
corrosive gas (NO+NO2) I advise you to let it run in a safe place or
outside, shelter from the rain.
Process :
The
principle is to produce nitric acid (HNO3), from the ambiant air, by
heating it to plasma, « near 3000°C » by using the
following reactions :
N2 + O2 ⟶ 2 NO, then 2 NO
+ O2 ⟶ 2 NO2
Who is able to react with water :
3 NO2 + H2O ⟶ 2 HNO3 + NO
I
strongly advise you to read some documents online, like the wikipedia
page or other sources.
The process
is very simple BUT inefficient and slow (especially for this little
kit).
You should reach near 15/25g of HNO3/KWH of energy
consumed.
It is not amazing, but if you are a little laboratory
and just need some bottles or you are just curious of the process,
with pedagogical views, it is interesting.
You will reach
a low concentration, probably never over 20 %, but enough to
reach azeotropic concentration (near 67%) with distillations.
Contents :
-
1m tube
PTFE 6x8mm
-
20Cm
tube
PTFE 8x10mm
- Glass
Flask
19/26mm arm side
-
Neon
transformer 60W
- 1
bubbler
CO2 35mm ceramic
- 1
pump
3,5W
- 2Pcs
washers
PP Tube
Gland
-
1
PTFE Roll
-
2
Naked
copper wire
20Cm + PTFE washers
machined.
-
1 « Y » connector
- 2
electric
switch connector
-
50-60Cm of
PVC
pipe,
flexible, by
4x6mm
- 1 EU
plug to be wired
-
1 Bromothymol
flask
+ 0,15g of
Bromothymol powder
-
1 PTFE washer
machined (stopper)
NB : The final bubble jar and the air tank reactor (ideally a 5 Liter PE can) are NOT included, you can find it easily.
PDF
manual link
:
https://pdfhost.io/v/ctcNixyG6_Birkeland_kit_50W_version_2022
Enjoy
and be careful with these chemicals, think about your safety and the
safety of others.